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Models
7725, 7725i, 9725, and 9725i Analytical Injectors
The
316 stainless steel models 7725 and 7725i, and PEEK models 9725
and 9725i are Rheodyne's most advanced manual sample injectors
for analytical HPLC. These dependable injectors are the
newer versions of the classic Rheodyne injector 7125 (page 7).
New specialized features include:
• The Rheodyne patented Make-Before-Break (MBB ™ ) architecture
allows continuous flow between LOAD and INJECT positions which
greatly reduces transient pressure shocks that disrupts your system.
See Figure 3.
• Wide, 30° port angles offer easier access to fittings using
the Rheodyne Wrench (Part # 6810 on page 20).
• Front-end pressure screw makes it easy to adjust and maintain
pressure.
• Capability of a reproducible 2 µL sample injection with a 2
µL internal sample loop.
• A built-in position sensing switch ("i" versions) provides the
chromatograph with a reproducible start signal.
Figure 3 illustrates the MBB valve design. In the LOAD position,
mobile phase flow from pump port to column port travels through
both the rotor seal groove and the MBB passage (Position A). As
the rotor seal grooves rotate to change from LOAD to INJECT, there
is continuous mobile phase flow through both one rotor seal groove
and the MBB passage (Position B) until the rotation stops and
both rotor seal grooves are connected by the loop. Sample flow
begins through the loop to the column just as all flow stops through
the MBB passage (Position C). Sample flow never enters the MBB
passage.
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The
injectors contain a patented Rheodyne needle port design that connects
the tip of the syringe needle directly to the sample loop ensuring
zero sample loss, no cross-contamination, and syringe accuracy.
These versatile front-loading injectors allow both partial-filling
method (reproducibility of 1.0% RSD) and complete-filling method
(reproducibility of 0.1% RSD). This dual mode capability varies
sample volumes desirable for your analytical analysis. See Tech
Tips #6 and 7 on pages 21 and 25. Flow switching occurs at a flat
interface between a polymeric rotor seal and a ceramic stator face
assembly in both the stainless steel and PEEK models. You can have
confidence in the long seal life of this genuine Rheodyne part combination.
A simple, three-step operation involves inserting the syringe into
the needle port while in the LOAD position and turning the handle
to INJECT. The sample is on its way through your system and when
the handle returns to LOAD, the injector is ready for the next injection.
A 20 µL sample loop is furnished and accessory loops and syringes
are listed on pages 20 and 22. See Table I in Introduction to Rheodyne
Manual Valves on page 3 for detailed specifications. |